Synthesis of gold nanoparticles on dextran for catalytic reduction of 4-nitrophenol
Vol. 128 No. 1C (2019), Original Article
Vol. 128 No. 1C (2019)

Synthesis of gold nanoparticles on dextran for catalytic reduction of 4-nitrophenol

Original Article
https://doi.org/10.26459/hueuni-jns.v128i1C.5329
Published 2019-07-24
Tran Van Quang
Universiy of Science, Hue University, 77 Nguyen Hue St., Hue, Vietnam
Phan Ha Nu Diem
University of Sciences, Hue University, 77 Nguyen Hue St., Hue, Vietnam
Ton Nu My Phuong
University of Sciences, Hue University, 77 Nguyen Hue St., Hue, Vietnam
Tran Thai Hoa
University of Sciences, Hue University, 77 Nguyen Hue St., Hue, Vietnam
PDF (Vietnamese)

How to Cite

1.
Quang TV, Diem PHN, Phuong TNM, Hoa TT. Synthesis of gold nanoparticles on dextran for catalytic reduction of 4-nitrophenol. hueuni-jns [Internet]. 2019Jul.24 [cited 2024Nov.23];128(1C):13-2. Available from: http://222.255.146.83/index.php/hujos-ns/article/view/5329
ACM ACS APA ABNT Chicago Harvard IEEE MLA Turabian Vancouver

Download Citation

Endnote/Zotero/Mendeley (RIS) BibTeX
Crossref
Scopus
Google Scholar
Europe PMC

Abstract

In this paper, gold nanoparticles (AuNps) were synthesized using the chemical reduction method with dextran as a reducing agent and protecting agent to form the AuNps/dextran material. The parameters affecting the synthesis of gold nanoparticles, such as chloroauric acid concentration, dextran concentration, temperature, time, and pH of the reaction system, were studied. The formation of Au nanoparticles and their morphology and structure were analyzed using UV-Vis spectroscopy, scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), transmission electron microscopy (TEM), X-ray diffraction (XRD), and Fourier-transform infrared spectroscopy (FT-IR). The catalytic activity of AuNPs for 4-nitrophenol reduction to 4-aminophenol with sodium borohydride as a reducing agent was also investigated.

https://doi.org/10.26459/hueuni-jns.v128i1C.5329
PDF (Vietnamese)

References

  1. Huang HJ, Yu C, Chang HC, Chiu KP, Ming Chen H, Liu RS, Tsai DP. Plasmonic optical properties of a single gold nano-rod. Optics Express.2007;15(12): 7132.
  2. Hien NQ, Phu DV, Lan NTK, Anh NT, Dung NX, Du BD, et al. Chế tạo vàng nano bằng phương pháp chiếu xạ. Vietnam Journal of Chemistry. 2009;47(2).
  3. Campbell CT, Sharp JC, Yao YX, Karp EM, Silbaugh TL. Insights into catalysis by gold nanoparticles and their support effects through surface science studies of model catalysts. Faraday Discussions. 2011; 152:227.
  4. Du J, Yue R, Ren F, Yao Z, Jiang F, Yang P, Du Y. Simultaneous determination of uric acid and dopamine using a carbon fiber electrode modified by layer-by-layer assembly of graphene and gold nanoparticles. Gold Bulletin. 2013;46(3):137-144.
  5. Kannan P, John SA. Determination of nanomolar uric and ascorbic acids using enlarged gold nanoparticles modified electrode. Analytical Biochemistry. 2009;386(1):65-72.
  6. Huang X, Neretina S, El-Sayed MA. Gold Nanorods: From Synthesis and Properties to Biological and Biomedical Applications. Advanced Materials. 2009 ;21(48):4880-4910.
  7. Wu H, Luo Y, Huang Y, Dong Q, Hou C, Huo D, Zhao J, Lei Y. A Simple SERS-Based Trace Sensing Platform Enabled by AuNPs-Analyte/AuNPs Double-Decker Structure on Wax-Coated Hydrophobic Surface. Frontiers in Chemistry. 2018;6.
  8. Cai W. Applications of gold nanoparticles in cancer nanotechnology. Nanotechnology, Science and Applications. 2008;1:17-32.
  9. Trung NC, Nguyệt TTM, Huấn NQ, Nghiễm LX, Thi ND, Chân ĐT, et al. Nghiên cứu công nghệ chế tạo và hoạt tính xúc tác của nano vàng trên chất mang Fe2O3. Vietnam Journal of Chemistry. 2007;45(6).
  10. Choofong S, Suwanmala P, Pasanphan W. Water-soluble chitosan-gold composite nanoparticles: Preparation by radiolysis method. ICCM International Conferences on Composite Materials. 2011.
  11. Bai L, Dong C, Zhang Y, Li W, Chen J. Comparative Studies on the Quick Recognition of Melamine Using Unmodified Gold Nanoparticles and p-Nitrobenzenesulfonic Grafted Silver Nanoparticles. Journal of the Chinese Chemical Society. 2011;58(7):846-852.
  12. Banoee M, Mokhtari Nori N, Akhavan Sepahi A, Fesharaki PJ, Ehsanfar Z, Khoshayand M, et al. The green synthesis of gold nanoparticles using the ethanol extract of black tea and its tannin free fraction. Iranian Journal of Materials Science and Engineering. 2010;7:48-53.
  13. Long NN, Vu LV, Kiem CD, Doanh SC, Nguyet CT, Hang PT, et al. Synthesis and optical properties of colloidal gold nanoparticles. Journal of Physics: Conference Series. 2009;187:012026.
  14. Kuroda K, Ishida T, Haruta M. Reduction of 4-nitrophenol to 4-aminophenol over Au nanoparticles deposited on PMMA. Journal of Molecular Catalysis A: Chemical. 2009;298(1-2):7-11.
  15. Macqueen A. Factors that Affect the Synthesis of Gold Nanorods. 2007.
  16. Busbee B, Obare S, Murphy C. An Improved Synthesis of High-Aspect-Ratio Gold Nanorods. Advanced Materials. 2003;15(5):414-416.
  17. Holden MS, Nick KE, Hall M, Milligan JR, Chen Q, Perry CC. Synthesis and catalytic activity of pluronic stabilized silver–gold bimetallic nanoparticles. RSC Adv.. 2014;4(94):52279-52288.
  18. Tang JQ, Zhang N, Man SQ. Green Synthesis of Monodispersity Gold Nanoparticles with Dextran. Key Engineering Materials. 2017;727:365-368.
  19. Liu J, Qin G, Raveendran P, Ikushima Y. Facile “Green” Synthesis, Characterization, and Catalytic Function of β-D-Glucose-Stabilized Au Nanocrystals. Chemistry - A European Journal. 2006 ;12(8):2131-2138.
  20. Goia DV. Preparation and formation mechanisms of uniform metallic particles in homogeneous solutions. Journal of Materials Chemistry. 2004;14(4):451.
  21. Park K. Synthesis, Characterization, and Self –Assembly of Size Tunable Gold Nanorods. Geor-gia Institute of Technology; 2006.
  22. Murugadoss A, Chattopadhyay A. Surface Area Controlled Differential Catalytic Activities of One-Dimensional Chain-like Arrays of Gold Nanoparticles. The Journal of Physical Chemistry C. 2008;112(30):11265-11271.
  23. Baruah B, Gabriel GJ, Akbashev MJ, Booher ME. Facile Synthesis of Silver Nanoparticles Stabilized by Cationic Polynorbornenes and Their Catalytic Activity in 4-Nitrophenol Reduction. Langmuir. 2013;29(13):4225-4234.
  24. Chiu C, Chung P, Lao K, Liao C, Huang MH. Facet-Dependent Catalytic Activity of Gold Nanocubes, Octahedra, and Rhombic Dodecahedra toward 4-Nitroaniline Reduction. The Journal of Physical Chemistry C. 2012;116(44):23757-23763.
  25. Panigrahi S, Basu S, Praharaj S, Pande S, Jana S, Pal A, Ghosh SK, Pal T. Synthesis and Size-Selective Catalysis by Supported Gold Nanoparticles: Study on Heterogeneous and Homogeneous Catalytic Process. The Journal of Physical Chemistry C. 2007;111(12):4596-4605.
Creative Commons License

This work is licensed under a Creative Commons Attribution-ShareAlike 4.0 International License.

Copyright (c) 2019 Array